Measurement and ab initio calculation of CSA/dipole-dipole cross-correlated relaxation provide insight into the mechanism of a H2-forming dehydrogenase.

نویسندگان

  • Stefan Bartoschek
  • Gerrit Buurman
  • Bernhard H Geierstanger
  • Jon Lapham
  • Christian Griesinger
چکیده

Using transferred cross-correlated relaxation and DFT calculations, the conformation of the relevant conformation of N5,N10-methylenetetrahydromethanopterin, a reaction intermediate bound to the 80 kD H2-forming N5,N10-methylenetetrahydromethanopterin dehydrogenase is determined. The conformation of the intermediate differs from the free form in solution and makes the reaction mechanism plausible.

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عنوان ژورنال:
  • Journal of the American Chemical Society

دوره 125 44  شماره 

صفحات  -

تاریخ انتشار 2003